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Operational control of supply lines erected by Lake Constance water supply association (BWV) 1974
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Print(0)
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Journal Article
Periodical, Full
Periodical, Abbrev.
WASSERWIRTSCHAFT
Pub Date Free Form
1974/
Volume
64
Issue
6
Start Page
167
Other Pages
173
Notes
Place of Publication
ISSN/ISBN
Accession Number
Language
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
In the years 1967-1971 the Zweckverband Bodensee Wasserversorgung (BWV) erected a second long distance water pipeline from the Bodensee to Stuttgart at a total expenditure of nearly 300 million DM. The article describes the supervisory remote control equipment with control panel and attached data processing plant delivered by Brown Boveri.
Descriptors
environmental health
Links
Book Title
BETRIEBSUBERWACHUNG DER VERSORGUNGSLEITUNGEN DES ZWECKVERBANDES BODENSEE WASSERVERSORGUNG
Database
Embase
Publisher
Data Source
Embase
Authors
Baensch,G., Muench,G.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Opinions about electronic cigarette use in smoke-free areas among U.S. Adults, 2012 2015 School of Public Health, Georgia State University, Atlanta, GA bmajeed1@student.gsu.edu.; School of Public Health, Georgia State University, Atlanta, GA.; School of Public Health, Georgia State University, Atlanta, GA.; School of Public Health, Georgia St
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Nicotine & tobacco research : official journal of the Society for Research on Nicotine and Tobacco
Periodical, Abbrev.
Nicotine Tob.Res.
Pub Date Free Form
Jun
Volume
17
Issue
6
Start Page
675
Other Pages
681
Notes
LR: 20160715; CI: (c) The Author 2014; GR: P50 DA036128/DA/NIDA NIH HHS/United States; GR: P50DA036128/DA/NIDA NIH HHS/United States; GR: R03 CA159909/CA/NCI NIH HHS/United States; GR: R21 CA180934/CA/NCI NIH HHS/United States; JID: 9815751; OID: NLM: PMC
Place of Publication
England
ISSN/ISBN
1469-994X; 1462-2203
Accession Number
PMID: 25358659
Language
eng
SubFile
Journal Article; Research Support, N.I.H., Extramural; Research Support, Non-U.S. Gov't; Research Support, U.S. Gov't, P.H.S.; IM
DOI
10.1093/ntr/ntu235 [doi]
Output Language
Unknown(0)
PMID
25358659
Abstract
INTRODUCTION: In the United States, electronic cigarettes (e-cigarettes) are currently unregulated, extensively marketed, and experiencing a rapid increase in use. The purpose of this study was to examine the opinions of U.S. adults about e-cigarette use in smoke-free public areas. METHODS: Data were obtained from the online HealthStyle survey administered to a probability sample of a nationally representative online panel. The study included 4,043U.S. adults, aged 18 years or older who responded to this question, "Do you think e-cigarette should be allowed to be used in public areas where tobacco smoking is prohibited?" Multinomial logistic regression analyses were used to examine opinions on e-cigarette use in smoke-free areas by sex, age, race/ethnicity, household income, education, census region, and cigarette smoking status and e-cigarette awareness and ever use. RESULTS: Overall, about 40% of adults were uncertain whether e-cigarettes should be allowed in smoke-free areas, 37% opposed, while 23% favored their use in smoke-free public places. Multinomial logistic regression analyses showed that adults who were aware, ever used e-cigarettes, and current cigarette smokers were more likely to express an "in favor" opinion than adults who expressed an uncertain opinion (don't know). CONCLUSION: Over 75% of U.S. adults reported uncertainty or disapproval of the use of e-cigarettes in smoke-free areas. Current cigarette smokers, adults aware or have ever used e-cigarettes were more supportive to exempting e-cigarettes from smoking restrictions. With impending regulation and the changing e-cigarette landscape, continued monitoring and research on public opinions about e-cigarette use in smoke-free places are needed.
Descriptors
Links
Book Title
Database
Publisher
. Published by Oxford University Press on behalf of the Society for Research on Nicotine and Tobacco
Data Source
Authors
Majeed,B.A., Dube,S.R., Sterling,K., Whitney,C., Eriksen,M.P.
Original/Translated Title
URL
Date of Electronic
20141030
PMCID
PMC4838050
Editors
Opioid antagonists for smoking cessation 2013 Center for Education in Family & Community Medicine, Stanford University, Stanford, California, USA. spdavid@stanford.edu.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
The Cochrane database of systematic reviews
Periodical, Abbrev.
Cochrane Database Syst.Rev.
Pub Date Free Form
6-Jun
Volume
(6):CD003086. doi
Issue
6
Start Page
CD003086
Other Pages
Notes
LR: 20160602; GR: P50 DA009253/DA/NIDA NIH HHS/United States; GR: P50 DA009253/DA/NIDA NIH HHS/United States; GR: R01 MH083684/MH/NIMH NIH HHS/United States; GR: R01 MH083684/MH/NIMH NIH HHS/United States; JID: 100909747; 0 (Narcotic Antagonists); 36B82AM
Place of Publication
England
ISSN/ISBN
1469-493X; 1361-6137
Accession Number
PMID: 23744347
Language
eng
SubFile
Journal Article; Meta-Analysis; Research Support, N.I.H., Extramural; Research Support, Non-U.S. Gov't; Review; IM
DOI
10.1002/14651858.CD003086.pub3 [doi]
Output Language
Unknown(0)
PMID
23744347
Abstract
BACKGROUND: The reinforcing properties of nicotine may be mediated through release of various neurotransmitters both centrally and systemically. People who smoke report positive effects such as pleasure, arousal, and relaxation as well as relief of negative affect, tension, and anxiety. Opioid (narcotic) antagonists are of particular interest to investigators as potential agents to attenuate the rewarding effects of cigarette smoking. OBJECTIVES: To evaluate the efficacy of opioid antagonists in promoting long-term smoking cessation. The drugs include naloxone and the longer-acting opioid antagonist naltrexone. SEARCH METHODS: We searched the Cochrane Tobacco Addiction Group Specialised Register for trials of naloxone, naltrexone and other opioid antagonists and conducted an additional search of MEDLINE using 'Narcotic antagonists' and smoking terms in April 2013. We also contacted investigators, when possible, for information on unpublished studies. SELECTION CRITERIA: We considered randomised controlled trials comparing opioid antagonists to placebo or an alternative therapeutic control for smoking cessation. We included in the meta-analysis only those trials which reported data on abstinence for a minimum of six months. We also reviewed, for descriptive purposes, results from short-term laboratory-based studies of opioid antagonists designed to evaluate psycho-biological mediating variables associated with nicotine dependence. DATA COLLECTION AND ANALYSIS: We extracted data in duplicate on the study population, the nature of the drug therapy, the outcome measures, method of randomisation, and completeness of follow-up. The main outcome measure was abstinence from smoking after at least six months follow-up in patients smoking at baseline. Abstinence at end of treatment was a secondary outcome. We extracted cotinine- or carbon monoxide-verified abstinence where available. Where appropriate, we performed meta-analysis, pooling risk ratios using a Mantel-Haenszel fixed-effect model. MAIN RESULTS: Eight trials of naltrexone met inclusion criteria for meta-analysis of long-term cessation. One trial used a factorial design so five trials compared naltrexone versus placebo and four trials compared naltrexone plus nicotine replacement therapy (NRT) versus placebo plus NRT. Results from 250 participants in one long-term trial remain unpublished. No significant difference was detected between naltrexone and placebo (risk ratio (RR) 1.00; 95% confidence interval (CI) 0.66 to 1.51, 445 participants), or between naltrexone and placebo as an adjunct to NRT (RR 0.95; 95% CI 0.70 to 1.30, 768 participants). The estimate was similar when all eight trials were pooled (RR 0.97; 95% CI 0.76 to 1.24, 1213 participants). In a secondary analysis of abstinence at end of treatment, there was also no evidence of any early treatment effect, (RR 1.03; 95% CI 0.88 to 1.22, 1213 participants). No trials of naloxone or buprenorphine reported abstinence outcomes. AUTHORS' CONCLUSIONS: Based on data from eight trials and over 1200 individuals, there was no evidence of an effect of naltrexone alone or as an adjunct to NRT on long-term smoking abstinence, with a point estimate strongly suggesting no effect and confidence intervals that make a clinically important effect of treatment unlikely. Although further trials might narrow the confidence intervals they are unlikely to be a good use of resources.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
David,S.P., Lancaster,T., Stead,L.F., Evins,A.E., Prochaska,J.J.
Original/Translated Title
URL
Date of Electronic
20130606
PMCID
PMC4038652
Editors
Opium, tobacco, and alcohol use in relation to oesophageal squamous cell carcinoma in a high-risk area of Iran 2008
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Br J Cancer
Periodical, Abbrev.
Br.J.Cancer
Pub Date Free Form
Volume
98
Issue
11
Start Page
1857
Other Pages
63
Notes
ID: 18475303
Place of Publication
ISSN/ISBN
Accession Number
Language
en
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
The very high incidence of oesophageal squamous cell carcinoma (ESCC) in Golestan Province in northeastern Iran was suggested by studies in the 1970s as partly due to opium use, which is not uncommon in this area, but based on limited numbers. From December 2003 to June 2007, we administered a validated structured questionnaire to 300 ESCC cases and 571 controls, matched on neighbourhood of residence, age (+/-2 years), and sex. We used conditional logistic regression models to calculate odds ratios (ORs) and 95% confidence intervals (95% CIs) adjusted for potential confounders. Compared with those who used neither tobacco nor opium, risk of ESCC was increased in those who used tobacco only (OR, 95% CI: 1.70, 1.05-2.73), in those who used opium only (2.12, 1.21-3.74), and in those who used both tobacco and opium (2.35, 1.50-3.67). All forms of tobacco use (cigarettes, hookah, and nass) were associated with higher ESCC risk. Similarly, use of both crude opium and other forms of opium were associated with higher risk. Alcohol consumption was seen in only 2% of the cases and 2% of the controls, and was not associated with ESCC risk.
Descriptors
Alcohol Drinking/adverse effects, Carcinoma, Squamous Cell/etiology, Esophageal Neoplasms/etiology, Opium/adverse effects, Smoking/adverse effects, Adult, Aged, Female, Humans, Male, Middle Aged, Mutagens/toxicity, Risk Factors
Links
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2410115/?tool=pubmed; http://dx.doi.org/10.1038/sj.bjc.6604369
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Nasrollahzadeh,D., Kamangar,F., Aghcheli,K., Sotoudeh,M., Islami,F., Abnet,C. C., Shakeri,R., Pourshams,A., Marjani,H. A., Nouraie,M., Khatibian,M., Semnani,S., Ye,W., Boffetta,P., Dawsey,S. M., Malekzadeh,R.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Opium: an emerging risk factor for gastric adenocarcinoma 2013
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Int J Cancer
Periodical, Abbrev.
Int.J.Cancer
Pub Date Free Form
Volume
133
Issue
2
Start Page
455
Other Pages
61
Notes
ID: 23319416
Place of Publication
ISSN/ISBN
Accession Number
Language
en
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
Opium use has been associated with higher risk of cancers of the esophagus, bladder, larynx, and lung; however, no previous study has examined its association with gastric cancer. There is also little information on the associations between hookah (water pipe) smoking or the chewing of tobacco products and the risk of gastric cancer. In a case-control study in Golestan Province of Iran, we enrolled 309 cases of gastric adenocarcinoma (118 noncardia, 161 cardia and 30 mixed-location adenocarcinomas) and 613 matched controls. Detailed information on long-term use of opium, tobacco products and other covariates were collected using structured and validated lifestyle and food frequency questionnaires. Odds ratios (ORs) and 95% confidence intervals (95% CIs) were obtained using conditional logistic regression models. Opium use was associated with an increased risk of gastric adenocarcinoma, with an adjusted OR (95% CI) of 3.1 (1.9-5.1), and this increased risk was apparent for both anatomic subsites (cardia and noncardia). There was a dose-response effect, and individuals with the highest cumulative opium use had the strongest association (OR: 4.5; 95% CI: 2.3-8.5). We did not find a statistically significant association between the use of any of the tobacco products and risk of gastric adenocarcinoma, overall or by anatomic subsite. We showed, for the first time, an association between opium use and gastric adenocarcinoma. Given that opium use is a traditional practice in many parts of the world, these results are of public health significance.
Descriptors
Links
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Shakeri,Ramin, Malekzadeh,Reza, Etemadi,Arash, Nasrollahzadeh,Dariush, Aghcheli,Karim, Sotoudeh,Masoud, Islami,Farhad, Pourshams,Akram, Pawlita,Michael, Boffetta,Paolo, Dawsey,Sanford M., Abnet,Christian C., Kamangar,Farin
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Opportunistic insights into occupational health hazards associated with waterpipe tobacco smoking premises in the United Kingdom 2015 Queen Mary, University of London, Barts and The London School of Medicine and Dentistry, Institute of Dentistry, London, UK E-mail : s.kassim@qmul.ac.uk.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Asian Pacific journal of cancer prevention : APJCP
Periodical, Abbrev.
Asian Pac.J.Cancer.Prev.
Pub Date Free Form
Volume
16
Issue
2
Start Page
621
Other Pages
626
Notes
JID: 101130625; 0 (Tobacco Smoke Pollution); 7U1EE4V452 (Carbon Monoxide); ppublish
Place of Publication
Thailand
ISSN/ISBN
1513-7368; 1513-7368
Accession Number
PMID: 25684497
Language
eng
SubFile
Journal Article; IM
DOI
Output Language
Unknown(0)
PMID
25684497
Abstract
BACKGROUND: Smokefree laws aim to protect employees and the public from the dangers of secondhand smoke. Waterpipe premises have significantly increased in number in the last decade, with anecdotal reports of poor compliance with the smokefree law. The literature is bereft of information pertaining to waterpipe premise employees. This study aimed to opportunistically gather knowledge about the occupational health hazards associated with working in waterpipe premises in London, England. MATERIALS AND METHODS: Employees from seven convenience-sampled, smokefree-compliant waterpipe premises in London were observed for occupational activities. Opportunistic carbon monoxide (CO) measurements were made among those with whom a rapport had developed. Observations were thematically coded and analysed. RESULTS: Occupational hazards mainly included environmental smoke exposure. Waterpipe-serving employees were required to draw several puffs soon after igniting the coals, thereby providing quality assurance of the product. Median CO levels were 27.5 ppm (range 21-55 ppm) among these employees. Self-reported employee health was poor, with some suggestion that working patterns and smoke exposure was a contributory factor. CONCLUSIONS: The smokefree law in England does not appear to protect waterpipe premise employees from high levels of CO. Continued concerns surrounding chronic smoke exposure may contribute to poor self-reported physical and mental wellbeing.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Al-Bakri,A., Jawad,M., Salameh,P., al'Absi,M., Kassim,S.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Opportunities for policy interventions to reduce youth hookah smoking in the United States 2012
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Prev Chronic Dis
Periodical, Abbrev.
Pub Date Free Form
Volume
9
Issue
Start Page
E165
Other Pages
E165
Notes
ID: 23153772
Place of Publication
ISSN/ISBN
Accession Number
Language
en
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
Preventing youth smoking initiation is a priority for tobacco control programs, because most adult tobacco smokers become addicted during adolescence. Interventions that restrict the affordability, accessibility, and marketing of cigarettes have been effective in reducing youth cigarette smoking. However, increasing numbers of youth are smoking tobacco using hookahs. Predictors of smoking tobacco with hookahs are the same as those for smoking cigarettes. Established interventions that curb youth cigarette smoking should therefore be effective in reducing hookah use. Potential policy interventions include equalizing tobacco tax rates for all tobacco types, requiring warning labels on hookah tobacco and accurate labeling of product contents, extending the cigarette flavoring ban to hookah tobacco, enacting smoke-free air laws and removing exemptions for hookah lounges, and expanding shipping restrictions on tobacco products.
Descriptors
Links
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Morris,Daniel S., Fiala,Steven C., Pawlak,Rebecca
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Optimal planning model for rehabilitation of water networks 2004 Kim, J.-H., Dept. of Civ. and Environ. Eng., Korea University, Seoul, South Korea
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Water Science and Technology: Water Supply
Periodical, Abbrev.
Water Sci.Technol.Water Supply
Pub Date Free Form
2004/
Volume
4
Issue
3
Start Page
133
Other Pages
147
Notes
Place of Publication
ISSN/ISBN
1606-9749
Accession Number
Language
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
An optimal planning model for rehabilitation of water networks is presented. Capital costs (replacement, rehabilitation and repairing costs), benefits (by the reduction of pumping cost and leakage cost), and hydraulic reliability are used for making an optimal decision for the rehabilitation plan of a water pipe network. KYPIPE is used for checking the hydraulic reliability. A multi-objective optimization model is successfully developed in this study. And the task is tackled using a new meta-heuristic algorithm, Harmony Search, for solving a large optimization problem to which conventional optimization techniques are poorly suited. Five different models with different objective functions are developed and tested according to various conditions considered in this study. These models provide more options for the rehabilitation of pipe network systems compared to previously suggested models in the literature.
Descriptors
algorithm, conference paper, cost, hydrology, reliability, theoretical model, water management, water supply
Links
Book Title
Database
Embase
Publisher
Data Source
Embase
Authors
Kim,J. -H, Baek,C. -W, Jo,D. -J, Kim,E. -S, Park,M. -J
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Optimization of a GC/MS procedure that uses parallel factor analysis for the determination of bisphenols and their diglycidyl ethers after migration from polycarbonate tableware 2013 Department of Chemistry, Faculty of Sciences, University of Burgos, Plaza Misael Banuelos s/n, 09001 Burgos, Spain.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Talanta
Periodical, Abbrev.
Talanta
Pub Date Free Form
15-Mar
Volume
106
Issue
Start Page
266
Other Pages
280
Notes
CI: Copyright (c) 2012; JID: 2984816R; 0 (Benzhydryl Compounds); 0 (Epoxy Compounds); 0 (Epoxy Resins); 0 (Phenols); 0 (Polycarboxylate Cement); 0 (bisphenol F diglycidyl ether); 25766-59-0 (polycarbonate); MLT3645I99 (bisphenol A); QD2C19044Z (4,4'-bisph
Place of Publication
Netherlands
ISSN/ISBN
1873-3573; 0039-9140
Accession Number
PMID: 23598127
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.talanta.2012.10.086 [doi]
Output Language
Unknown(0)
PMID
23598127
Abstract
Bisphenol A (BPA), bisphenol F (BPF) and their corresponding diglycidyl ethers (BADGE and BFDGE) are simultaneously determined using a programmed-temperature vaporizer-gas chromatography/mass spectrometry (PTV-GC/MS) system. BPA is used in the production of polycarbonate (PC), whereas BADGE and BFDGE are for manufacturing epoxy resins. Several food alerts caused by the migration of this kind of substances from contact food materials have led to the harmonization of the European legislation in Commission Regulation (EU) No. 10/2011, in force from 14 January 2011. In consequence, the use of BPA has been prohibited in the manufacture of plastic infant feeding bottles from 1 May 2011 and from 1 June 2011 regarding the placing on the market and importation into the European Union. Recently, the French Parliament has decreed that the presence of BPA in any food containers will be banned. Similarly, the use and/or presence of BFDGE are not allowed. In this work, a GC/MS method has been developed for the simultaneous determination of BPF, BPA, BFDGE and BADGE. For each one of the I samples that are analyzed, the abundance of J characteristic m/z ratios is recorded at K times around the retention time of each peak, so a data tensor of dimension IxJxK is obtained for every analyte. The decomposition of this tensor by means of parallel factor analysis (PARAFAC) enables to: (a) identify unequivocally each analyte according to the maximum permitted tolerances for relative ion intensities, and (b) quantify each analyte, even in the presence of coeluents. This identification, based on the mass spectrum and the retention time, guarantees the specificity of the analysis. This specificity could fail if the total ion chromatogram (TIC) is considered when there is poor resolution between some peaks or whether interferents coelute. With the aim of studying the effect of shortening the time of the analysis on the quality of the determinations while maintaining the specificity of the identifications, two of the heating ramps in the oven temperature program are changed according to a two-level factorial design. Each analyte is identified by means of a PARAFAC decomposition of a data tensor obtained from several concentration levels, in such a way that five figures of merit are calculated for each experiment of the design. The analysis of these figures of merit for the 16 objects (4 compoundsx4 heating ramps) using principal component analysis (PCA) shows that the shortest temperature program should be considered, since this is the one the best figures of merit for BPA and BFDGE (both banned) are achieved with. At these conditions and with probabilities of false positive and false negative fixed at 0.05, values of detection capability (CCbeta) between 2.65 and 4.71 mug L(-1) when acetonitrile is the injection solvent, and between 1.97 and 5.53 mug L(-1) when acetone, are obtained. This GC/MS method has been applied to the simultaneous determination of BPF, BPA, BFDGE and BADGE in food simulant D1 (ethanol-H2O, 1:1 v/v), which had been previously in contact with PC tableware for 24h at 70 degrees C and then pretreated by a solid-phase extraction (SPE) step. The migration of BPA from the new PC containers analyzed is confirmed, and values between 104.67 and 181.46 mug L(-1) (0.73 and 1.27 mug L(-1) after correction) of BPA have been estimated. None of the results obtained exceeds the specific migration limit of 600 mug L(-1) established by law for BPA in plastic food materials different from PC infant feeding bottles. Severe problems of coelution of interferents have been overcome using PARAFAC decompositions in the analysis of these food simulant samples.
Descriptors
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Oca,M.L., Ortiz,M.C., Herrero,A., Sarabia,L.A.
Original/Translated Title
URL
Date of Electronic
20121102
PMCID
Editors
Optimization of a novel method for determination of benzene, toluene, ethylbenzene, and xylenes in hair and waste water samples by carbon nanotubes reinforced sol-gel based hollow fiber solid phase microextraction and gas chromatography using factorial ex 2011 Department of Chemistry, Payame Noor University, Tehran, Iran. zarrin eshaghi@yahoo.com
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of chromatography.A
Periodical, Abbrev.
J.Chromatogr.A
Pub Date Free Form
27-May
Volume
1218
Issue
21
Start Page
3400
Other Pages
3406
Notes
LR: 20151119; CI: Copyright (c) 2011; JID: 9318488; 0 (Benzene Derivatives); 0 (Nanotubes, Carbon); 0 (Water Pollutants, Chemical); 451W47IQ8X (Sodium Chloride); 2011/01/02 [received]; 2011/03/16 [revised]; 2011/03/17 [accepted]; 2011/04/12 [aheadofprint]
Place of Publication
Netherlands
ISSN/ISBN
1873-3778; 0021-9673
Accession Number
PMID: 21489540
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.chroma.2011.03.043 [doi]
Output Language
Unknown(0)
PMID
21489540
Abstract
A novel design of solid phase microextraction fiber containing carbon nanotube reinforced sol-gel which was protected by polypropylene hollow fiber (HF-SPME) was developed for pre-concentration and determination of BTEX in environmental waste water and human hair samples. The method validation was included and satisfying results with high pre-concentration factors were obtained. In the present study orthogonal array experimental design (OAD) procedure with OA(16) (4(4)) matrix was applied to study the effect of four factors influencing the HF-SPME method efficiency: stirring speed, volume of adsorption organic solvent, extraction and desorption time of the sample solution, by which the effect of each factor was estimated using individual contributions as response functions in the screening process. Analysis of variance (ANOVA) was employed for estimating the main significant factors and their percentage contributions in extraction. Calibration curves were plotted using ten spiking levels of BTEX in the concentration ranges of 0.02-30,000ng/mL with correlation coefficients (r) 0.989-0.9991 for analytes. Under the optimized extraction conditions, the method showed good linearity (0.3-20,000ng/L), repeatability, low limits of detections (0.49-0.7ng/L) and excellent pre-concentration factors (185-1872). The best conditions which were estimated then applied for the analysis of BTEX compounds in the real samples.
Descriptors
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Es'haghi,Z., Ebrahimi,M., Hosseini,M.S.
Original/Translated Title
URL
Date of Electronic
20110412
PMCID
Editors