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Application of counter-current chromatography as a new pretreatment method for the determination of polycyclic aromatic hydrocarbons in environmental water 2012 Beijing Technology and Business University, School of Food and Chimerical Engineering, Beijing, PR China. caoxl@th.btbu.edu.cn
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of separation science
Periodical, Abbrev.
J.Sep.Sci.
Pub Date Free Form
Feb
Volume
35
Issue
4
Start Page
596
Other Pages
601
Notes
LR: 20150325; CI: Copyright (c) 2012; GR: Z99 HL999999/Intramural NIH HHS/United States; JID: 101088554; 0 (Polycyclic Hydrocarbons, Aromatic); 0 (Water Pollutants, Chemical); NIHMS339391; OID: NLM: NIHMS339391; OID: NLM: PMC3270381; ppublish
Place of Publication
Germany
ISSN/ISBN
1615-9314; 1615-9306
Accession Number
PMID: 22282420
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1002/jssc.201100852 [doi]
Output Language
Unknown(0)
PMID
22282420
Abstract
Counter-current chromatography (CCC) was investigated as a new sample pretreatment method for the determination of trace polycyclic aromatic hydrocarbons (PAHs) in water environmental samples. The experiment was performed with a non-aqueous binary two-phase solvent system composed of n-heptane and acetonitrile. The CCC column was first filled with the upper stationary phase, and then a large volume of water sample was pumped into the column while the CCC column was rotated at 1600 rpm. Finally, the trace amounts of PAHs extracted and enriched in the stationary phase were eluted out by the lower mobile phase and determined by gas chromatography-flame ionization detector (GC-FID) or gas chromatography-mass spectrometry (GC-MS). The enrichment and cleanup of PAHs can be fulfilled online by this method with high recoveries (84.1-103.2%) and good reproducibility (RSDs: 4.9-12.2%) for 16 EPA PAHs under the optimized CCC pretreatment conditions. This method has been successfully applied to determine PAHs in lake water where 8 PAHs were detected in the concentration of 40.9-89.9 ng/L. The present method is extremely suitable for the preparation of large volume of environmental water sample for the determination of trace amounts of organic pollutants including PAHs as studied in this paper.
Descriptors
Links
Book Title
Database
Publisher
WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Data Source
Authors
Cao,X., Yang,C., Pei,H., Li,X., Xu,X., Ito,Y.
Original/Translated Title
URL
Date of Electronic
PMCID
PMC3270381
Editors
Application of hydraulic transients for leak detection in water supply systems 2004 Covas, D., Civil Eng. Dept., Instituto Superior Técnico, 1049-001 Lisbon, Portugal
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Water Science and Technology: Water Supply
Periodical, Abbrev.
Water Sci.Technol.Water Supply
Pub Date Free Form
2004/
Volume
4
Issue
6-May
Start Page
365
Other Pages
374
Notes
Place of Publication
ISSN/ISBN
1606-9749
Accession Number
Language
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
The current paper reports the investigation of two transient-based techniques for leak detection in water pipe systems using physical data collected in the laboratory and in quasi-field conditions. The first is the analysis of the leak reflected wave during a transient event and the second is inverse transient analysis (ITA). This was approached through the development of an inverse transient analysis tool and the collection of transient data for the testing and validation of this model. Two experimental programmes were carried out at Imperial College and in cooperation with Thames Water for the validation and testing of these techniques. Evaluation of the presence, location and size of leaks was carried out using the collected data. Transient-based techniques have been shown to be successful in the detection and location of leaks and leak location uncertainties depended on the leak size and location, flow regime and location where the transient event was generated. These leak detection methods are very promising for identifying the general area of the trunk main with leakage, and can be combined with other leak location techniques (e.g. acoustic equipment) to more precisely pinpoint the leak position. Transient-based techniques are particularly important for the diagnosis, monitoring and control of existing water supply systems, not only to detect leaks, but also to better understand the causes of pipe bursts and accidents, particularly when these are due to natural transient events.
Descriptors
acoustics, analytic method, conference paper, cooperation, data analysis, equipment design, flow kinetics, hydraulic conductivity, inverse transient analysis, laboratory diagnosis, physical chemistry, tube, water supply
Links
Book Title
Database
Embase
Publisher
Data Source
Embase
Authors
Covas,D., Ramos,H., Graham,N., Maksimovic,C.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Application of ultrasound-assisted emulsification microextraction based on applying low-density organic solvent for the determination of organochlorine pesticides in water samples 2012 Department of Chemistry, National University of Singapore, 3 Science Drive 3, Singapore 117543, Singapore.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of chromatography.A
Periodical, Abbrev.
J.Chromatogr.A
Pub Date Free Form
24-Aug
Volume
1252
Issue
Start Page
67
Other Pages
73
Notes
LR: 20151119; CI: Copyright (c) 2012; JID: 9318488; 0 (Hydrocarbons, Chlorinated); 0 (Octanes); 0 (Pesticides); 0 (Water Pollutants, Chemical); 451W47IQ8X (Sodium Chloride); 540-84-1 (2,2,4-trimethylpentane); 2012/04/17 [received]; 2012/06/14 [revised]; 2
Place of Publication
Netherlands
ISSN/ISBN
1873-3778; 0021-9673
Accession Number
PMID: 22771061
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.chroma.2012.06.065 [doi]
Output Language
Unknown(0)
PMID
22771061
Abstract
In this study, a polyethylene Pasteur pipette-based ultrasound-assisted emulsification microextraction (USAEME) applying low-density organic solvent was successfully developed for the extraction of trace levels of organochlorine pesticides (OCPs) in water samples and followed by gas chromatography-mass spectrometry (GC-MS) analysis. In this approach, a polyethylene Pasteur squeeze-type pipette was employed as a convenient extraction device and ultrasound radiation was applied to accelerate the emulsification of low-density organic solvent in aqueous solutions to enhance the microextraction efficiency of OCPs in water samples. Thirty microliters of extraction solvent (isooctane), of lower density than water, were injected into the aqueous sample solution held in the pipette. The latter was then immersed in an ultrasound water bath to form an emulsion. After 30s extraction, phase separation was achieved by centrifugation. The upper layer (isooctane) was collected and analyzed by GC-MS. No disperser solvent was required in this procedure. Significantly, fast analysis and high extraction efficiency were achieved. Another feature of the procedure was the use of the pipette as the extraction device, which permitted less dense than water organic solvent to be used as extraction solvent. This method broadens the applicability of USAEME to a wider range of solvent. Additionally, carry-over problems were avoided with the use of the disposable pipette. Parameters affecting the efficiency of polyethylene Pasteur pipette-based USAEME, such as the extraction solvent, extraction solvent volume, extraction and centrifugation time, ionic strength and extraction temperature were investigated. Under the optimum conditions, the proposed method provided good enrichment factors (EFs) in the range of 128 and 328, with relative standard deviations (RSDs) ranging from 2.7% to 12.4%. The limits of detection were in the range of 0.8 and 10ng/L depending on the analytes. The linearities were between 0.01 and 50mug/L for hexachlorobenzene, dieldrin, endrin and o,p'-DDD, 0.05-25mug/L for heptachlor, and 0.005-50mug/L for p,p'-DDE. Finally, the polyethylene Pasteur pipette-based USAEME was successfully used for the fast determination of OCPs in river and tap water samples. The proposed method provides a simple, convenient, rapid, sensitive, cost-effective, and environmentally friendly process for the determination of OCPs in water samples.
Descriptors
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Zhang,Y., Lee,H.K.
Original/Translated Title
URL
Date of Electronic
20120626
PMCID
Editors
Aptitude aérobie sous-maximale et qualité de vie des fumeurs exclusifs de narguilé 2010
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Rev Mal Respir
Periodical, Abbrev.
Rev.Mal.Respir.
Pub Date Free Form
Volume
27
Issue
5
Start Page
489
Other Pages
95
Notes
ID: 20569882
Place of Publication
ISSN/ISBN
Accession Number
Language
fr
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
BACKGROUND: It is well known that oxidative stress is increased significantly by regular water-pipe smoking (WPS). This could lead to muscle dysfunction and thus to impairments of exercise and quality of life (QOL). Considering the impressive number of WP smokers, we intend to investigate the potential effect of WPS on submaximal exercise capacity and QOL. AIMS: (1). To evaluate the submaximal exercise capacity by the 6-minutes walking test (6-MWT). (2). To compare the deficiency, incapacity and QOL data of exclusive WPS with those of two control groups (never smokers and exclusive cigarette smokers). (3). To determine the factors influencing the 6-minutes walk distance (6-MWD) of WPS subjects. METHODS: A multicentre study including 180 exclusive WPS > or =5 WP-year] men aged > or =40 years. Cigar or cigarette smoking, contraindications to the 6-MWT or cortico-steroid therapy will be exclusion criteria. QOL evaluation, spirometry, electrocardiogram and two 6-MWT will be performed. Signs of exercise impairment will be: 6-MWD or =5/10, haemoglobin saturation fall > or =5 points. Data from WPS subjects will be compared with those from 90 never smoking subjects and 90 exclusives cigarettes smokers. EXPECTED RESULTS: (1). WPS will affect significantly the submaximal exercise capacity. (2). Resting spirometric, 6-MWT and QOL data of exclusive WPS subjects will be significantly reduced compared to never smoking subjects. (3). The 6-MWD's of exclusive WPS subjects will be significantly influenced by cumulative WP consumption, by resting spirometric data, by obesity and by physical activity score.
Descriptors
Exercise Tolerance, Quality of Life, Smoking/physiopathology, Adult, Cross-Sectional Studies, Humans, Male, Middle Aged, Multicenter Studies as Topic, Water
Links
http://dx.doi.org/10.1016/j.rmr.2010.03.009
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Ben Saad,H., Babba,M., Boukamcha,R., Latiri,I., Knani,J., Slama,R., Bougmiza,I., Zbidi,A., Tabka,Z.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Arab-American adolescent tobacco use: four pilot studies 2003 Wayne State University, Detroit, MI 48202, USA. vrice@wayne.edu
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Preventive medicine
Periodical, Abbrev.
Prev.Med.
Pub Date Free Form
Nov
Volume
37
Issue
5
Start Page
492
Other Pages
498
Notes
LR: 20151119; JID: 0322116; ppublish
Place of Publication
United States
ISSN/ISBN
0091-7435; 0091-7435
Accession Number
PMID: 14572433
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
S0091743503001750 [pii]
Output Language
Unknown(0)
PMID
14572433
Abstract
OBJECTIVES: Four pilot studies were conducted to determine the (1) current tobacco use patterns and predictors among 14- to 18-year-old Arab-American youths; (2) psychometric properties of study measures (English and Arabic); (3) cultural appropriateness of Project Toward No Tobacco (TNT) for intervention; (4) accessible population for a longitudinal study. METHODS: Three studies were descriptive and one used a pretest-posttest design. From four Pilot Focus groups (N = 28 smokers) key tobacco use themes emerged along with information on study measures and the Project TNT intervention; Pilot Intervention tested the tailored Project TNT intervention with 9 Arab-American teens; Pilot Clinic (N = 44) determined the characteristics of the accessible teen health clinic population; and Pilot School (N = 119) obtained tobacco use data only. RESULTS: From Pilot Focus seven themes (being cool, "nshar ma'a al shabab" [hanging out with the guys], present [time] orientation, smoking feels and tastes good, keeps your mind off trouble, easy to get, and (many) "barriers to quitting") emerged from the data. In the Pilot Intervention a 37.5% cessation rate was found. In the Pilot Clinic study, 24% males and 17% females smoked. The current smoking rate in the Pilot School (N = 119) sample was 17%; 34% admitted to having ever smoked (even a puff). Significant predictors for current tobacco use included poor grades, stress, having many family members and peers who smoke, being exposed to many hours of smoking each day, receiving offers of tobacco products, advertising and mail, and believing that tobacco can help one to make friends. CONCLUSIONS: The four pilots contributed unique and essential knowledge for designing a longitudinal clinical trial on tobacco use by Arab-American adolescents.
Descriptors
Adolescent, Adolescent Behavior/ethnology, Arabs/ethnology, Attitude to Health/ethnology, Cultural Characteristics, Female, Focus Groups, Friends, Health Knowledge, Attitudes, Practice, Humans, Male, Needs Assessment, Peer Group, Pilot Projects, Predictive Value of Tests, Psychology, Adolescent, Psychometrics, Qualitative Research, Risk Factors, Sample Size, Smoking/ethnology/prevention & control, Smoking Cessation/ethnology/methods, Surveys and Questionnaires/standards, United States
Links
Book Title
Database
Publisher
Data Source
Authors
Rice,V. H., Templin,T., Kulwicki,A.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Arab-American Hookah Smokers: Initiation, and Pros and Cons of Hookah Use 2015 Center for Behavioral Epidemiology and Community Health (CBEACH), San Diego State University Research Foundation, San Diego, CA, USA. nadakassem@hotmail.com.; Center for Behavioral Epidemiology and Community Health (CBEACH), San Diego State University Res
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
American Journal of Health Behavior
Periodical, Abbrev.
Am.J.Health Behav.
Pub Date Free Form
Sep
Volume
39
Issue
5
Start Page
680
Other Pages
697
Notes
JID: 9602338; ppublish
Place of Publication
United States
ISSN/ISBN
1945-7359; 1087-3244
Accession Number
PMID: 26248178
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.5993/AJHB.39.5.10 [doi]
Output Language
Unknown(0)
PMID
26248178
Abstract
OBJECTIVES: To examine initiation, pros and cons of hookah tobacco smoking among Arab Americans. METHODS: In this descriptive cross-sectional study, we recruited a community-based convenience sample of 458 adult Arab-American hookah smokers, mean age 28.4 years, who completed self-administered questionnaires. RESULTS: Irrespective of sex, most participants initiated hookah tobacco use by young adulthood in private homes or hookah lounges influenced by friends and family. Women initiated hookah use later than men. Ever dual smokers (hookah smokers who ever smoked a cigarette) initiated hookah use later than cigarettes; however, early hookah initiators
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Kassem,N.O., Kassem,N.O., Jackson,S.R., Daffa,R.M., Liles,S., Hovell,M.F.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Architecture, influencing factors, and sensitivity to antifungal agents of Candida biofilm 2002 Department of Dermatology, PUMC Hospital, CAMS, PUMC, Beijing 100730, China. sunqnzhy@yahoo.com
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Zhongguo yi xue ke xue yuan xue bao.Acta Academiae Medicinae Sinicae
Periodical, Abbrev.
Zhongguo Yi Xue Ke Xue Yuan Xue Bao
Pub Date Free Form
Aug
Volume
24
Issue
4
Start Page
385
Other Pages
388
Notes
LR: 20131121; JID: 8006230; 0 (Antifungal Agents); 304NUG5GF4 (Itraconazole); 7XU7A7DROE (Amphotericin B); 8VZV102JFY (Fluconazole); ppublish
Place of Publication
China
ISSN/ISBN
1000-503X; 1000-503X
Accession Number
PMID: 12905659
Language
chi
SubFile
English Abstract; Journal Article; IM
DOI
Output Language
Unknown(0)
PMID
12905659
Abstract
OBJECTIVE: To establish a model of Candida biofilm and to explore its characteristics, ultrastructure, influences by saliva and serum, and sensitivity to antifungal agents. METHODS: Evaluations of the in vitro growth kinetics, influences by saliva and serum, and sensitivity to antifungal agents of Candida biofilm were performed with the abated tetrazolium salt XTT method on a 96-well microtire petri dish. The ultrastructure of Candida biofilm was observed under Confocal Laser Scanning Microscope (CLSM). RESULTS: The bioactivity of Candida biofilm increased with culturing time and serum could obviously increase the action of biofilm. The Candida biofilm was significantly resistant to routine antifungal agents. CONCLUSION: The Candida cells adhered in biofilms are significantly different in morphology from those in suspension and are resistant to routine antifungal agents such as Amphotericine B, Fluconazole and Itraconazole.
Descriptors
Amphotericin B/pharmacology, Antifungal Agents/pharmacology, Biofilms/drug effects, Candida/drug effects/ultrastructure, Drug Resistance, Fungal, Fluconazole/pharmacology, Itraconazole/pharmacology, Microbial Sensitivity Tests, Microscopy, Confocal
Links
Book Title
Database
Publisher
Data Source
Authors
Sun,Q. N., Fang,K.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Are experimental smokers different from their never-smoking classmates? A multilevel analysis of Canadian youth in grades 9 to 12 2014 School of Public Health and Health Systems, University of Waterloo, Waterloo, Ontario, Canada.; School of Public Health and Health Systems, University of Waterloo, Waterloo, Ontario, Canada; Propel Centre for Population Health Impact, University of Waterl
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Chronic diseases and injuries in Canada
Periodical, Abbrev.
Chronic Dis.Inj.Can.
Pub Date Free Form
Jul
Volume
34
Issue
3-Feb
Start Page
121
Other Pages
131
Notes
JID: 101556266; OTO: NOTNLM; ppublish
Place of Publication
Canada
ISSN/ISBN
1925-6523; 1925-6515
Accession Number
PMID: 24991775
Language
eng; fre
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
Output Language
Unknown(0)
PMID
24991775
Abstract
INTRODUCTION: Understanding the characteristics of experimental smoking among youth is critical for designing prevention programs. This study examined which student- and school-level factors differentiated experimental smokers from never smokers in a nationally representative sample of Canadian students in grades 9 to 12. METHODS: School-level data from the 2006 Canadian Census and one built environment characteristic (tobacco retailer density) were linked with data from secondary school students from the 2008-2009 Canadian Youth Smoking Survey and examined using multilevel logistic regression analyses. RESULTS: Experimental smoking rates varied across schools (p
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Kaai,S.C., Manske,S.R., Leatherdale,S.T., Brown,K.S., Murnaghan,D.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Are primary health care providers prepared to implement an anti-smoking program in Syria? 2011
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Patient Educ Couns
Periodical, Abbrev.
Patient Educ.Couns.
Pub Date Free Form
Volume
85
Issue
2
Start Page
201
Other Pages
5
Notes
ID: 21168300
Place of Publication
ISSN/ISBN
Accession Number
Language
en
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
OBJECTIVE: To document primary health care (PHC) providers' tobacco use, and how this influences their smoking cessation practices and attitudes towards tobacco-control policies. METHODS: Anonymous questionnaires were distributed to PHC providers in 7 randomly selected PHC centers in Aleppo, Syria. RESULTS: All PHC providers completed the questionnaires (100% response rate). A quarter of these providers smoke cigarettes and more than 10% smoke waterpipes. Physicians who smoke were less likely to advise patients to quit (OR=0.29; 95% CI, 0.09-0.95), assess their motivation to quit (OR=0.13, 95% CI=0.02-0.72), or assist them in quitting (OR=0.24, 95% CI=0.06-0.99). PHC providers who smoke were less likely to support a ban on smoking in PHC settings (68.2% vs. 89.1%) and in enclosed public places (68.2% vs. 86.1%) or increases in the price of tobacco products (43.2% vs. 77.4%) (P<0.01 for all comparisons). CONCLUSIONS: Smoking, including waterpipe, continues to be widespread among PHC providers in Syria and will negatively influence implementation of anti-smoking program in PHC settings. PRACTICE IMPLICATIONS: Smoking awareness and cessation interventions targeted to PHC providers, and training programs to build providers' competency in addressing their patients' smoking is crucial in Syria.
Descriptors
Attitude of Health Personnel, Nurses/psychology, Physicians/psychology, Primary Health Care, Smoking Cessation, Smoking/prevention & control, Smoking/psychology, Adult, Chi-Square Distribution, Female, Humans, Logistic Models, Male, Prevalence, Smoking/epidemiology, Questionnaires, Syria/epidemiology
Links
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3074023/?tool=pubmed; http://dx.doi.org/10.1016/j.pec.2010.11.011
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Asfar,Taghrid, Al-Ali,Radwan, Ward,Kenneth D., Vander Weg,Mark,W., Maziak,Wasim
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Are quit attempts among U.S. female nurses who smoke different from female smokers in the general population? An analysis of the 2006/2007 tobacco use supplement to the current population survey 2012 School of Nursing, University of California, Los Angeles, 700 Tiverton Ave, Los Angeles, CA 90095, USA. lsarna@sonnet.ucla.edu
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
BMC women's health
Periodical, Abbrev.
BMC Womens Health
Pub Date Free Form
19-Mar
Volume
12
Issue
Start Page
4
Other Pages
12/4/6874
Notes
LR: 20150225; JID: 101088690; OID: NLM: PMC3328253; 2011/10/31 [received]; 2012/03/19 [accepted]; 2012/03/19 [aheadofprint]; epublish
Place of Publication
England
ISSN/ISBN
1472-6874; 1472-6874
Accession Number
PMID: 22429917
Language
eng
SubFile
Comparative Study; Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1186/1472-6874-12-4 [doi]
Output Language
Unknown(0)
PMID
22429917
Abstract
BACKGROUND: Smoking is a significant women's health issue. Examining smoking behaviors among occupational groups with a high prevalence of women may reveal the culture of smoking behavior and quit efforts of female smokers. The purpose of this study was to examine how smoking and quitting characteristics (i.e., ever and recent quit attempts) among females in the occupation of nursing are similar or different to those of women in the general population. METHODS: Cross-sectional data from the Tobacco Use Supplement of the Current Population Survey 2006/2007 were used to compare smoking behaviors of nurses (n = 2, 566) to those of non-healthcare professional women (n = 93, 717). Smoking characteristics included years of smoking, number of cigarettes, and time to first cigarette with smoking within the first 30 minutes as an indicator of nicotine dependence. Logistic regression models using replicate weights were used to determine correlates of ever and previous 12 months quit attempts. RESULTS: Nurses had a lower smoking prevalence than other women (12.1% vs 16.6%, p
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Sarna,L., Bialous,S.A., Nandy,K., Yang,Q.
Original/Translated Title
URL
Date of Electronic
20120319
PMCID
PMC3328253
Editors