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Title Pub Year Author Sort descending SearchLink
Determinants of tobacco use among youths in Isfahan, Iran 2007 Kelishadi, R., Isfahan Cardiovascular Research Center (WHO - Collaborating Center in EMR), Isfahan University of Medical Sciences, Isfahan, Iran
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
International Journal of Public Health
Periodical, Abbrev.
Int.J.Public Health
Pub Date Free Form
/
Volume
52
Issue
3
Start Page
173
Other Pages
179
Notes
Place of Publication
ISSN/ISBN
1661-8556; 1420-911X
Accession Number
Language
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
Objective: To determine potential factors that may result in motivating the youths to adopt smoking behaviour Method: This cross-sectional study was conducted on 210 smoking and 217 non-smoking youths, aged 12-20 years. Results: The average age of starting cigarette and water pipe smoking was 14.5 ± 2.4 and 11.2 ± 1.5 years, respectively. The first experience with water pipe occurred mostly in the traditional teahouses for girls (54.8 %), and in family parties (48.2 %) for boys. In both genders, the first place of cigarette smoking was at friends' parties (56.8 % for boys, and 52.1 % for girls) and then followed by traditional teahouses (43.2 % for boys, and 47.9 % for girls). The most common reasons youths have picked up cigarette smoking were mainly to attract attention from friends, family inattention and poverty. Meanwhile, nearly all water pipe smokers reported using it for fun. The strongest predictors of smoking among boys were respectively father's occupation, having a smoking mother, and the number of smoking peers, whereas among girls, these factors were respectively having a smoking mother, frequenting traditional teahouses, and the number of smoking peers. Lower education of fathers and divorce among parents increased the probability of smoking in both genders, especially girls. School/ work failure, as well as troubled relationship with parents and siblings were the other significant predictors of smoking in both genders, notably in girls. Conclusion: Public health control measures should be adopted not only to curtail cigarette use, but also to address water-pipe use. Preventive measures should be regarded as a high priority for socio-economically disadvantaged families. © Birkhäuser Verlag, Basel 2007.
Descriptors
academic failure, adolescent, adult, article, child behavior, child parent relation, smoking, controlled study, divorce, educational status, family relation, female, gender bias, human, Iran, male, maternal smoking, motivation, peer group, poverty, priority journal, probability, public health, risk factor, school child, sibling relation, smoking cessation program
Links
Book Title
Database
Embase; MEDLINE
Publisher
Data Source
Embase
Authors
Kelishadi,R., Mokhtari,M. R., Tavasoli,A. A., Khosravi,A., Ahangar-Nazari,I., Sabet,B., Kazemi,A., Amini,A.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Waterpipe tobacco use among Iranian university students: correlates and perceived reasons for use 2011 Kerman University of Medical Sciences, Kerman, Iran.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
The international journal of tuberculosis and lung disease : the official journal of the International Union against Tuberculosis and Lung Disease
Periodical, Abbrev.
Int.J.Tuberc.Lung Dis.
Pub Date Free Form
Jun
Volume
15
Issue
6
Start Page
844
Other Pages
847
Notes
LR: 20151119; JID: 9706389; 059QF0KO0R (Water); ppublish
Place of Publication
France
ISSN/ISBN
1815-7920; 1027-3719
Accession Number
PMID: 21575309
Language
eng
SubFile
Journal Article; Multicenter Study; IM
DOI
10.5588/ijtld.10.0744 [doi]
Output Language
Unknown(0)
PMID
21575309
Abstract
SETTING: Waterpipe smoking is becoming a global health crisis among youth. OBJECTIVE: To identify the prevalence of waterpipe use among Iranian university students and to explore perceived reasons for use. METHODS: A random sample of 1024 university students at two major universities in South Iran was enrolled in the study. A three-part questionnaire (baseline data, tobacco smoking status and perceived reasons for waterpipe use) was used. Students filled out the self-administered questionnaire in their classrooms. RESULTS: The prevalence of waterpipe smoking in the respondents' lifetime and in the last 30 days was 42.5% and 18.7%, respectively. The mean age at initiation of waterpipe smoking was 16.3 +/- 3.2 years. Ever smoking was positively associated with age and male sex, whereas no association was found regarding marital status. The highest odds of lifetime waterpipe smoking were observed in students with close friends who smoked the waterpipe (5.94, 95%CI 4.26-8.30). The most important perceived reason for waterpipe smoking as stated by students was enjoyment (55.8%). CONCLUSION: Given the alarming prevalence of waterpipe smoking, preventive measures should be adopted among university students taking into account the influence of peers, siblings and parents in the lessening social tolerance of waterpipe smoking.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Sabahy,A.R., Divsalar,K., Bahreinifar,S., Marzban,M., Nakhaee,N.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
C18 functionalized graphene oxide as a novel coating for solid-phase microextraction 2012 Key Laboratory for Natural Medicine of Gansu Province, Chinese Academy of Sciences, Lanzhou Institute of Chemical Physics, Lanzhou, China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of separation science
Periodical, Abbrev.
J.Sep.Sci.
Pub Date Free Form
Jun
Volume
35
Issue
12
Start Page
1531
Other Pages
1537
Notes
CI: (c) 2012; JID: 101088554; 0 (Oxides); 0 (Polycyclic Hydrocarbons, Aromatic); 0 (Water Pollutants, Chemical); 7782-42-5 (Graphite); ppublish
Place of Publication
Germany
ISSN/ISBN
1615-9314; 1615-9306
Accession Number
PMID: 22740264
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1002/jssc.201200124 [doi]
Output Language
Unknown(0)
PMID
22740264
Abstract
A novel C18 functionalized graphene oxide (GO) coated solid-phase microextraction fiber was prepared by a novel protocol. Based on the strong van der Waals interaction present in GO and abundant oxygenous groups in GO sheets, a simple layer-by-layer self-assembly method was used in the preparation process and then C18 was successfully self-assembled on GO via C-O-Si bonding. Coupled with gas chromatography, extraction performance of the fiber was tested with polycyclic aromatic hydrocarbons (PAHs) as model analytes. The fiber not only exhibited excellent extraction efficiency and selectivity, but also showed many advantages including high rigidity, long service life and well stability toward organic solvent, acidic and alkali solutions, and high temperature. The relative standard deviations for single-fiber repeatability and fiber-to-fiber reproducibility were less than 7.26 and 17.25%, respectively. The detection limits to the PAHs were less than 0.08 mug L(-1) and the calibration curves were linear in a wide range for all analytes. The as-established Solid-phase microextraction GC method was also successfully used for determination of PAHs in two real water samples.
Descriptors
Links
Book Title
Database
Publisher
WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Data Source
Authors
Xu,L., Feng,J., Liang,X., Li,J., Jiang,S.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
A novel multiwalled carbon nanotubes bonded fused-silica fiber for solid phase microextraction-gas chromatographic analysis of phenols in water samples 2009 Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Talanta
Periodical, Abbrev.
Talanta
Pub Date Free Form
15-May
Volume
78
Issue
3
Start Page
929
Other Pages
935
Notes
LR: 20131121; JID: 2984816R; 0 (Nanotubes, Carbon); 0 (Phenols); 059QF0KO0R (Water); 7631-86-9 (Silicon Dioxide); 2008/11/04 [received]; 2008/12/23 [revised]; 2008/12/30 [accepted]; 2009/01/20 [aheadofprint]; ppublish
Place of Publication
England
ISSN/ISBN
1873-3573; 0039-9140
Accession Number
PMID: 19269452
Language
eng
SubFile
Evaluation Studies; Journal Article; IM
DOI
10.1016/j.talanta.2008.12.061 [doi]
Output Language
Unknown(0)
PMID
19269452
Abstract
The present work reports on the synthesis of chemically bonded multiwalled carbon nanotubes (MWCNTs)/fused-silica fibers and their use in solid phase microextraction of seven phenols from water samples coupled with gas chromatography (GC). The synthetic strategy was verified by infrared (IR) spectroscopy and field emission scanning electron microscopy. Adsorption factors (pH, ionic strength, stirring rate, adsorption time and temperature) and desorption factors (time and temperature) of the fibers were systematically investigated. Detection limits to seven phenols were less than 0.05 microg L(-1), and their calibration curves were all linear (R(2)> or =0.9984) in the range from 0.05 to 5000 microg L(-1). This method was then utilized to analyze two real water samples from Yellow River and sanitary wastewater, resulting in satisfactory results. Compared with normal solid phase materials, this MWCNTs-bonded fused-silica fibers showed a number of advantages: wide linear range and low detection limit for extracting phenols couple with GC, and good stability in acid, alkali, organic solvents and at high temperature.
Descriptors
Chromatography, Gas/methods, Nanotubes, Carbon, Phenols/analysis, Silicon Dioxide, Solid Phase Microextraction/methods, Water/analysis
Links
Book Title
Database
Publisher
Data Source
Authors
Liu,H., Li,J., Liu,X., Jiang,S.
Original/Translated Title
URL
Date of Electronic
20090120
PMCID
Editors
Polymeric ionic liquid modified stainless steel wire as a novel fiber for solid-phase microextraction 2013 Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of separation science
Periodical, Abbrev.
J.Sep.Sci.
Pub Date Free Form
Jan
Volume
36
Issue
2
Start Page
369
Other Pages
375
Notes
CI: (c) 2012; JID: 101088554; 0 (Ionic Liquids); 0 (Polymers); 0 (Water Pollutants, Chemical); 12597-68-1 (Stainless Steel); 2012/07/07 [received]; 2012/08/28 [revised]; 2012/09/11 [accepted]; ppublish
Place of Publication
Germany
ISSN/ISBN
1615-9314; 1615-9306
Accession Number
PMID: 23335459
Language
eng
SubFile
Evaluation Studies; Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1002/jssc.201200644 [doi]
Output Language
Unknown(0)
PMID
23335459
Abstract
A polymeric ionic liquid modified stainless steel wire for solid-phase microextraction was reported. Mercaptopropyl-functionalized stainless steel wire that was formed by co-condensation of tetramethoxysilane and 3-mercaptopropyltrimethoxysilane via a sol-gel process, which is followed by in situ surface radical chain-transfer polymerization of 1-vinyl-3-octylimidazolium hexafluorophosphate to result in polymeric ionic liquid modified stainless steel wire. The fiber surface was characterized by field emission scanning electron microscope equipped with energy dispersive X-ray analysis. Coupled with GC, extraction performance of the fiber was tested with phenols and polycyclic aromatic hydrocarbons as model analytes. Effects of extraction and desorption conditions were investigated systematically in our work. RSDs for single-fiber repeatability and fiber-to-fiber reproducibility were less than 7.34 and 16.82%, respectively. The calibration curves were linear in a wide range for all analytes and the detection limits were in the range of 10-60 ng L(-1) . Two real water samples from the Yellow River and local waterworks were applied to test the as-established solid-phase microextraction-GC method with the recoveries of samples spiked at 10 mug L(-1) ranged from 83.35 to 119.24%. The fiber not only exhibited excellent extraction efficiency, but also very good rigidity, stability and durability.
Descriptors
Links
Book Title
Database
Publisher
WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Data Source
Authors
Xu,L., Jia,J., Feng,J., Liu,J., Jiang,S.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Graphene oxide bonded fused-silica fiber for solid-phase microextraction-gas chromatography of polycyclic aromatic hydrocarbons in water 2012 Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, P. R. China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of separation science
Periodical, Abbrev.
J.Sep.Sci.
Pub Date Free Form
Jan
Volume
35
Issue
1
Start Page
93
Other Pages
100
Notes
CI: Copyright (c) 2012; JID: 101088554; 0 (Oxides); 0 (Polycyclic Hydrocarbons, Aromatic); 0 (Water Pollutants, Chemical); 7631-86-9 (Silicon Dioxide); 7782-42-5 (Graphite); 2011/07/14 [received]; 2011/09/02 [revised]; 2011/09/26 [accepted]; 2011/11/28 [a
Place of Publication
Germany
ISSN/ISBN
1615-9314; 1615-9306
Accession Number
PMID: 22125228
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1002/jssc.201100612 [doi]
Output Language
Unknown(0)
PMID
22125228
Abstract
A novel chemically bonded graphene oxide/fused-silica fiber was prepared and applied in solid-phase microextraction of six polycyclic aromatic hydrocarbons from water samples coupled with gas chromatography. It exhibited high extraction efficiency and excellent stability. Effects of extraction time, extraction temperature, ionic strength, stirring rate and desorption conditions were investigated and optimized in our work. Detection limits to the six polycyclic aromatic hydrocarbons were less than 0.08 mug/L, and their calibration curves were all linear (R(2)>/=0.9954) in the range from 0.05 to 200 mug/L. Single fiber repeatability and fiber-to-fiber reproducibility were less than 6.13 and 15.87%, respectively. This novel fiber was then utilized to analyze two real water samples from the Yellow River and local waterworks, and the recoveries of samples spiked at 1 and 10 mug/L ranged from 84.48 to 118.24%. Compared with other coating materials, this graphene oxide-coated fiber showed many advantages: wide linear range, low detection limit, and good stability in acid, alkali, organic solutions and at high temperature.
Descriptors
Links
Book Title
Database
Publisher
WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Data Source
Authors
Xu,L., Feng,J., Li,J., Liu,X., Jiang,S.
Original/Translated Title
URL
Date of Electronic
20111128
PMCID
Editors
A novel TiO2 nanotube array/Ti wire incorporated solid-phase microextraction fiber with high strength, efficiency and selectivity 2010 Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, No. 18 Tianshui Road, Lanzhou 730000, China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of chromatography.A
Periodical, Abbrev.
J.Chromatogr.A
Pub Date Free Form
19-Mar
Volume
1217
Issue
12
Start Page
1898
Other Pages
1903
Notes
LR: 20131121; CI: Copyright 2010; JID: 9318488; 0 (Alkanes); 0 (Polycyclic Hydrocarbons, Aromatic); 059QF0KO0R (Water); 15FIX9V2JP (titanium dioxide); D1JT611TNE (Titanium); 2009/12/04 [received]; 2010/01/21 [revised]; 2010/01/27 [accepted]; 2010/02/02 [a
Place of Publication
Netherlands
ISSN/ISBN
1873-3778; 0021-9673
Accession Number
PMID: 20153861
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.chroma.2010.01.080 [doi]
Output Language
Unknown(0)
PMID
20153861
Abstract
A novel solid-phase microextraction (SPME) fiber is fabricated through the anodization of Ti wire substrates in an electrolyte containing ethylene glycol and NH(4)F. By a combination of field emission scanning electron microscope and X-ray photoelectron spectroscope studies, it is shown that perpendicularly orientated and well-aligned TiO(2) nanotubes are grown in situ on the Ti wire substrate. The SPME fiber coupled with gas chromatograph (GC) is then used to extract polycyclic aromatic hydrocarbons (PAHs), anilines, phenols, and alkanes from standard and real water samples, and exhibits high selectivity for PAHs. After the optimization of adsorption factors (pH, ionic strength, time and temperature) and desorption factors (time and temperature) of the SPME fiber for PAHs, the limit of detection (LOD) of less than 0.1 microg L(-1) is achieved, and the calibration curves are all linear (R(2)> or =0.9898) in the range from 0.1 to 1000 microg L(-1). Beyond that, the SPME fiber has high strength, large surface area, good stability at high temperature and in acid and alkali solutions, and long service life, making it have strong application potentials in the selective extraction of PAHs from complex samples at trace levels.
Descriptors
Adsorption, Alkanes/isolation & purification, Chromatography, Gas, Electrodes, Limit of Detection, Nanotubes/chemistry/ultrastructure, Osmolar Concentration, Photoelectron Spectroscopy, Polycyclic Hydrocarbons, Aromatic/isolation & purification, Solid Phase Microextraction/instrumentation, Surface Properties, Temperature, Time Factors, Titanium/chemistry, Water/chemistry
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Liu,H., Wang,D., Ji,L., Li,J., Liu,S., Liu,X., Jiang,S.
Original/Translated Title
URL
Date of Electronic
20100202
PMCID
Editors
Highly selective and effective solid phase microextraction of benzoic acid esters using ionic liquid functionalized multiwalled carbon nanotubes-doped polyaniline coating 2016 Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of Education), College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, PR China; Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials &
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of chromatography.A
Periodical, Abbrev.
J.Chromatogr.A
Pub Date Free Form
11-Mar
Volume
1437
Issue
Start Page
1
Other Pages
7
Notes
CI: Copyright (c) 2016; JID: 9318488; 0 (Aniline Compounds); 0 (Esters); 0 (Ionic Liquids); 0 (Nanotubes, Carbon); 0 (Water Pollutants, Chemical); 0 (polyaniline); 8SKN0B0MIM (Benzoic Acid); OTO: NOTNLM; 2015/09/30 [received]; 2016/01/04 [revised]; 2016/0
Place of Publication
Netherlands
ISSN/ISBN
1873-3778; 0021-9673
Accession Number
PMID: 26852620
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.chroma.2016.01.072 [doi]
Output Language
Unknown(0)
PMID
26852620
Abstract
The present work reports the electrochemical fabrication of an ionic liquid functionalized multiwalled carbon nanotubes-polyaniline (MWCNT@IL/PANI) nanocomposite coating and its application in the headspace-solid phase microextraction (HS-SPME) and gas chromatography (GC) determination of benzoic acid esters (i.e., methyl benzoate, ethyl benzoate, propyl benzoate and butyl benzoate). The MWCNTs was firstly functionalized with amine-terminated IL (MWCNT@IL) through chemical reduction, and then was doped in PANI during the electropolymerization of aniline. The resulting coating was characterized by infrared spectroscopy, field emission scanning electron microscopy and thermo gravimetry. It showed net-like structure and had high thermal stability (up to 330 degrees C). Furthermore, it presented high selectivity for the four benzoic acid esters and thus suited for their HS-SPME-GC determination. Results showed that under optimized extraction conditions, the detection limits were less than 6.1ngL(-1) (S/N=3) and the linear detection ranges were 0.012-50mugL(-1) (R>/=0.9957) for these analytes. The relative standard deviations (RSDs) were lower than 6.4% for five successive measurements with one fiber, and the RSDs for fiber-to-fiber were 4.4-9.6% (n=5). The developed method was successfully applied to the determination of these benzoic acid esters in perfume samples.
Descriptors
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Ai,Y., Wu,M., Li,L., Zhao,F., Zeng,B.
Original/Translated Title
URL
Date of Electronic
20160202
PMCID
Editors
Sorptive extraction using polydimethylsiloxane/metal-organic framework coated stir bars coupled with high performance liquid chromatography-fluorescence detection for the determination of polycyclic aromatic hydrocarbons in environmental water samples 2014 Key Laboratory of Analytical Chemistry for Biology and Medicine, Ministry of Education, Department of Chemistry, Wuhan University, Wuhan 430072, China.; Key Laboratory of Analytical Chemistry for Biology and Medicine, Ministry of Education, Department of
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Journal of chromatography.A
Periodical, Abbrev.
J.Chromatogr.A
Pub Date Free Form
22-Aug
Volume
1356
Issue
Start Page
45
Other Pages
53
Notes
CI: Copyright (c) 2014; JID: 9318488; 0 (Coordination Complexes); 0 (Dimethylpolysiloxanes); 0 (Polycyclic Hydrocarbons, Aromatic); 0 (Water Pollutants, Chemical); 63148-62-9 (baysilon); CPD4NFA903 (Aluminum); OTO: NOTNLM; 2014/04/08 [received]; 2014/06/1
Place of Publication
Netherlands
ISSN/ISBN
1873-3778; 0021-9673
Accession Number
PMID: 25001335
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1016/j.chroma.2014.06.062 [doi]
Output Language
Unknown(0)
PMID
25001335
Abstract
In this work, metal-organic frameworks (MOFs, Al-MIL-53-NH(2)) were synthesized via the hydrothermal method, and novel polydimethylsiloxane/metal-organic framework (PDMS/MOFs, PDMS/Al-MIL-53-NH(2))-coated stir bars were prepared by the sol-gel technique. The preparation reproducibility of the PDMS/MOFs-coated stir bar was good, with relative standard deviations (RSDs) ranging from 4.8% to 14.9% (n=7) within one batch and from 6.2% to 16.9% (n=6) among different batches. Based on this fact, a new method of PDMS/MOFs-coated stir bar sorptive extraction (SBSE) and ultrasonic-assisted liquid desorption (UALD) coupled with high performance liquid chromatography-fluorescence detection (HPLC-FLD) was developed for the determination of polycyclic aromatic hydrocarbons (PAHs) in environmental water samples. To obtain the best extraction performance for PAHs, several parameters affecting SBSE, such as extraction time, stirring rate, and extraction temperature, were investigated. Under optimal experimental conditions, wide linear ranges and good RSDs (n=7) were obtained. With enrichment factors (EFs) of 16.1- to 88.9-fold (theoretical EF, 142-fold), the limits of detection (LODs, S/N=3) of the developed method for the target PAHs were found to be in the range of 0.05-2.94 ng/L. The developed method was successfully applied to the analysis of PAHs in Yangtze River and East Lake water samples.
Descriptors
Links
Book Title
Database
Publisher
Elsevier B.V
Data Source
Authors
Hu,C., He,M., Chen,B., Zhong,C., Hu,B.
Original/Translated Title
URL
Date of Electronic
20140624
PMCID
Editors
Boron nitride nanotubes as novel sorbent for solid-phase microextraction of polycyclic aromatic hydrocarbons in environmental water samples 2014 Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Shandong Academy of Sciences, Jinan, Shandong, China.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Analytical and bioanalytical chemistry
Periodical, Abbrev.
Anal.Bioanal Chem.
Pub Date Free Form
Sep
Volume
406
Issue
24
Start Page
5751
Other Pages
5754
Notes
LR: 20160512; JID: 101134327; 0 (Boron Compounds); 0 (Polycyclic Hydrocarbons, Aromatic); 0 (Water Pollutants, Chemical); 2U4T60A6YD (boron nitride); 2014/04/28 [received]; 2014/07/14 [accepted]; 2014/07/08 [revised]; 2014/07/25 [aheadofprint]; ppublish
Place of Publication
Germany
ISSN/ISBN
1618-2650; 1618-2642
Accession Number
PMID: 25059725
Language
eng
SubFile
Evaluation Studies; Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.1007/s00216-014-8032-0 [doi]
Output Language
Unknown(0)
PMID
25059725
Abstract
Boron nitride nanotube (BNNT) is a novel material that shows potential ability in capturing organic pollutants. In this study, BNNTs fixed on a stainless steel fiber by a sol-gel technique were used as sorbent for solid-phase microextraction. Five polycyclic aromatic hydrocarbons with different numbers of aromatic rings were selected as target analysts. Gas chromatography coupled with tandem mass spectrometry was used for detection and quantitative determination. Under optimized conditions, the experimental results show a wide range of linearity (1 to 1,000 ng L(-1)), less than 10.1 % repeatability of relative standard deviation, and low detection limits (0.08 to 0.39 ng L(-1)). In addition, the fabricated fiber offered good thermal and chemical stability. The proposed method was successfully applied for the analysis of real water samples, and satisfactory results were obtained with relative recoveries ranging from 80.2 to 116.8 %. The results demonstrated that BNNTs could be used as sorbent for the analysis of environmental pollutants at trace levels.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Fu,M., Xing,H., Chen,X., Zhao,R., Zhi,C., Wu,C.L.
Original/Translated Title
URL
Date of Electronic
20140725
PMCID
Editors