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Ethyl 2-[4-(morpholin-4-yl)phen-yl]-1-[3-(2-oxopyrrolidin-1-yl)prop-yl]-1H-1,3-benzimid azole-5-carboxyl-ate monohydrate 2012 Institute for Research in Molecular Medicine, Universiti Sains Malaysia, Minden 11800, Penang, Malaysia.
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Journal Article
Periodical, Full
Acta crystallographica.Section E, Structure reports online
Periodical, Abbrev.
Acta Crystallogr.Sect.E.Struct.Rep.Online
Pub Date Free Form
1-Oct
Volume
68
Issue
Pt 10
Start Page
o2967
Other Pages
8
Notes
LR: 20130304; JID: 101089178; OID: NLM: PMC3470336; 2012/08/29 [received]; 2012/09/14 [accepted]; 2012/09/22 [epublish]; ppublish
Place of Publication
United States
ISSN/ISBN
1600-5368; 1600-5368
Accession Number
PMID: 23125749
Language
eng
SubFile
Journal Article
DOI
10.1107/S1600536812039268 [doi]
Output Language
Unknown(0)
PMID
23125749
Abstract
The asymmetric unit of the title compound, C(27)H(32)N(4)O(4).H(2)O, contains two independent benzimidazole-5-carboxyl-ate mol-ecules and two water mol-ecules. In both main mol-ecules, the pyrrolidine rings are in an envelope conformation with a methyl-ene C atom as the flap. The morpholine rings adopt chair conformations. Both benzimidazole rings are essentially planar, with maximum deviations of 0.008 (1) A, and form dihedral angles of 37.65 (6) and 45.44 (6) degrees with the benzene rings. In one mol-ecule, an intra-molecular C-Hcdots, three dots, centeredO hydrogen bond forms an S(7) ring motif. In the crystal, O-Hcdots, three dots, centeredO and O-Hcdots, three dots, centeredN hydrogen bonds connect pairs of main mol-ecules and pairs of water mol-ecules into two independent centrosymmetric four-compoment aggregates. These aggregates are connect by C-Hcdots, three dots, centeredO hydrogen bonds leading to the formation of a three-dimensional network, which is stabilized by C-Hcdots, three dots, centeredpi interactions.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Yoon,Y.K., Ali,M.A., Choon,T.S., Arshad,S., Razak,I.A.
Original/Translated Title
URL
Date of Electronic
20120922
PMCID
PMC3470336
Editors
Ethyl 2-[2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)hydrazin-1-yl]-4-methyl- 1,3-thia-zole-5-carboxyl-ate di-methyl-formamide monosolvate 2013 Department of Chemistry, Annamalai University, Annamalainagar 608 002, Chidambaram, Tamil Nadu, India.; Department of Chemistry, Annamalai University, Annamalainagar 608 002, Chidambaram, Tamil Nadu, India.
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Print(0)
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Journal Article
Periodical, Full
Acta crystallographica.Section E, Structure reports online
Periodical, Abbrev.
Acta Crystallogr.Sect.E.Struct.Rep.Online
Pub Date Free Form
18-Dec
Volume
70
Issue
Pt 1
Start Page
o68
Other Pages
9
Notes
LR: 20140217; JID: 101089178; OID: NLM: PMC3914099; 2014/01/01 [ecollection]; 2013/11/16 [received]; 2013/12/11 [accepted]; 2013/12/18 [epublish]; epublish
Place of Publication
United States
ISSN/ISBN
1600-5368; 1600-5368
Accession Number
PMID: 24527004
Language
eng
SubFile
Journal Article
DOI
10.1107/S1600536813033540 [doi]
Output Language
Unknown(0)
PMID
24527004
Abstract
In the title mol-ecule, C27H30N4O2S.C3H7NO, the fused piperidine and cyclo-hexane rings adopt a twin chair conformation and the phenyl groups occupy equatorial sites. The phenyl rings make a dihedral angle of 40.74 (2) degrees . In the crystal, the di-methyl-formamide solvent mol-ecule is connected to the main mol-ecule by an N-Hcdots, three dots, centeredO hydrogen bond. An additional N-Hcdots, three dots, centeredO hydrogen bond connects mol-ecules into chains along [100]. Pairs of weak C-Hcdots, three dots, centeredO hydrogen bonds connect inversion-related chains. The ethyl group was refined as disordered over two sets of sites with an occupancy ratio of 0.660 (17):0.340 (17).
Descriptors
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Book Title
Database
Publisher
Data Source
Authors
Jothivel,S., Kabilan,S.
Original/Translated Title
URL
Date of Electronic
20131218
PMCID
PMC3914099
Editors
Ethyl 2-[({[4-amino-5-cyano-6-(methyl-sulfan-yl)pyridin-2-yl]carbamo-yl}meth-yl)sulfan- yl]acetate monohydrate 2014 Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.; Department of Chemistry, Tulane University, New Orleans, LA 70118, USA.; Chemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, E
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Acta crystallographica.Section E, Structure reports online
Periodical, Abbrev.
Acta Crystallogr.Sect.E.Struct.Rep.Online
Pub Date Free Form
4-Jun
Volume
70
Issue
Pt 7
Start Page
o745
Other Pages
6
Notes
LR: 20140829; JID: 101089178; OID: NLM: PMC4120541; 2014/07/01 [ecollection]; 2014/05/27 [received]; 2014/05/29 [accepted]; 2014/06/04 [epublish]; epublish
Place of Publication
United States
ISSN/ISBN
1600-5368; 1600-5368
Accession Number
PMID: 25161542
Language
eng
SubFile
Journal Article
DOI
10.1107/S1600536814012495 [doi]
Output Language
Unknown(0)
PMID
25161542
Abstract
The title compound, C13H16N4O3S2.H2O, crystallizes in a 'folded' conformation with the ester group lying over the carbamoyl moiety, with one solvent water mol-ecule. The mol-ecular conformation is stabilized by an intra-molecular C-Hcdots, three dots, centeredO hydrogen bond, and an N-Hcdots, three dots, centeredO hydrogen-bonding inter-action involving the lattice water mol-ecule. The packing involves N-Hcdots, three dots, centeredN, N-Hcdots, three dots, centeredO, O-Hcdots, three dots, centeredN and O-Hcdots, three dots, centeredO hydrogen bonds and consists of tilted layers running approximately parallel to the c axis, with the ester groups on the outer sides of the layers and with channels running parallel to (101).
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Akkurt,M., Mague,J.T., Mohamed,S.K., Hussein,B.R., Albayati,M.R.
Original/Translated Title
URL
Date of Electronic
20140604
PMCID
PMC4120541
Editors
Ethyl 1-(2-bromo-propano-yl)-4-hydr-oxy-2,6-diphenyl-1,2,5,6-tetra-hydro-pyridine-3-car boxylate 2009
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
Acta crystallographica.Section E, Structure reports online
Periodical, Abbrev.
Acta Crystallogr.Sect.E.Struct.Rep.Online
Pub Date Free Form
27-Jun
Volume
65
Issue
Pt 7
Start Page
o1708
Other Pages
9
Notes
LR: 20130329; JID: 101089178; OID: NLM: PMC2969390; 2009/06/16 [received]; 2009/06/22 [accepted]; 2009/06/27 [epublish]; epublish
Place of Publication
England
ISSN/ISBN
1600-5368; 1600-5368
Accession Number
PMID: 21582960
Language
eng
SubFile
Journal Article
DOI
10.1107/S1600536809023836 [doi]
Output Language
Unknown(0)
PMID
21582960
Abstract
The title compound, C(23)H(24)BrNO(4), crystallizes with two independent mol-ecules per asymmetric unit. The methyl group of the ethoxy-carbonyl unit is disordered over two positions, with occupancies of 0.715 (12) and 0.285 (12) in one of the independent mol-ecules, and 0.529 (11) and 0.471 (11) in the other mol-ecule. In one of the independent mol-ecules, the tetra-hydro-pyridine ring adopts a half-chair conformation, while in the other it is in a distorted envelope conformation. In each independent mol-ecule, an intra-molecular O-Hcdots, three dots, centeredO hydrogen bond generates an S(6) ring motif. The two independent mol-ecules are linked via C-Hcdots, three dots, centeredO hydrogen bonds, forming a chain along the c axis.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Aridoss,G., Gayathri,D., Velmurugan,D., Kim,M. S., Jeong,Y. T.
Original/Translated Title
URL
Date of Electronic
20090627
PMCID
PMC2969390
Editors
Ethnicity and waterpipe smoking among US students 2012 Institute of Community Health, College of Pharmacy, University of Houston, Houston, Texas 77030, USA. smabughosh@uh.edu
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
The international journal of tuberculosis and lung disease : the official journal of the International Union against Tuberculosis and Lung Disease
Periodical, Abbrev.
Int.J.Tuberc.Lung Dis.
Pub Date Free Form
Nov
Volume
16
Issue
11
Start Page
1551
Other Pages
1557
Notes
JID: 9706389; 2012/09/18 [aheadofprint]; ppublish
Place of Publication
France
ISSN/ISBN
1815-7920; 1027-3719
Accession Number
PMID: 23006908
Language
eng
SubFile
Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
10.5588/ijtld.12.0152 [doi]
Output Language
Unknown(0)
PMID
23006908
Abstract
OBJECTIVES: To examine the effect of ethnicity on waterpipe smoking among college students. DESIGN: A cross-sectional study utilized data from University of Houston students through an online survey (n = 2334) from March to April 2011. The survey included questions on demographic characteristics (sex, age, race/ethnicity), tobacco use experience, risk perception, social acceptability and popularity. Multivariate logistic regression was used to determine predictors of waterpipe use with three outcomes: ever-use vs. no use, past-year use vs. no use and past-month use vs. no use. RESULTS: Half of the sample had previously smoked tobacco using a waterpipe, approximately a third in the past year and 12.5% in the past month. Significant predictors included Middle Eastern ethnicity, Middle Eastern friend, past cigarette or cigar use. Perception of harm was associated with less use in the ever-use model, while perceived addictiveness, social acceptability and popularity of waterpipes were predictors in all models. CONCLUSION: Our findings underscore the importance of developing culturally appropriate interventions to control waterpipe smoking among Middle Eastern Americans and those of Indian/Pakistani descent to curb further spread in US society, and highlight the importance of developing interventions that target the perceived addictiveness, social acceptability and popularity of waterpipe smoking.
Descriptors
Links
Book Title
Database
Publisher
Data Source
Authors
Abughosh,S., Wu,I.H., Peters,R.J., Hawari,F., Essien,E.J.
Original/Translated Title
URL
Date of Electronic
20120918
PMCID
Editors
Ethnic differences in reported smoking behaviors in face-to-face and telephone interviews 2004 Israel Center for Disease Control, Ministry of Health, Tel Hashomer, Israel. ornaepel@research.haifa.ac.il
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
European journal of epidemiology
Periodical, Abbrev.
Eur.J.Epidemiol.
Pub Date Free Form
Volume
19
Issue
7
Start Page
679
Other Pages
686
Notes
LR: 20071115; JID: 8508062; ppublish
Place of Publication
Netherlands
ISSN/ISBN
0393-2990; 0393-2990
Accession Number
PMID: 15461199
Language
eng
SubFile
Journal Article; IM
DOI
Output Language
Unknown(0)
PMID
15461199
Abstract
Different modes of gathering data on self-reported health measures and self-reported risk factors are used frequently in research. However, data on the influence of the mode of collection of data on self-reporting are limited. The aim of the study was to identify associations between the mode of data collection and self-reported smoking in two distinct ethnic groups, Jews and Arabs in Israel. During the last 2 years, data were collected in two national surveys regarding the smoking behaviors of Jews and Arabs in Israel. In the telephone surveys 4713 Israeli residents were interviewed and in the face-to-face interviewees 3239 people were interviewed. The interviewees were between the ages 25 and 64. There was no significant difference in smoking rates between face-to-face interviews and telephone interviews among Jewish men or women after adjusting for other variables associated with smoking. However, there was a difference between the two methods of data collection in the Arab population also after the adjustment. In this group, respondents tended to report more often being a smoker in the face-to-face interviews. This was especially apparent in Arab women. There was no significant difference in the reported number of cigarettes smoked in the two modes of data collection. In Arabs compared to Jews there is a significant difference between reporting smoking during a telephone interview and a face-to-face interview. The mode of data collection can affect comparisons between different groups.
Descriptors
Adult, Arabs, Female, Humans, Interviews as Topic, Israel, Jews, Male, Middle Aged, Smoking/ethnology, Tobacco
Links
Book Title
Database
Publisher
Data Source
Authors
Baron-Epel,O., Haviv-Messika,A., Green,M. S., Kalutzki,D. N.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Ethnic differences in cigarette smoking among adolescents: a comparison of Jews and Arabs in Jerusalem 2001 Pediatric Respiratory Medicine Unit, Department of Pediatrics, Shaare Zedek Medical Center (affiliated to Hebrew University-Hadassah Medical School), Jerusalem, Israel.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
The Israel Medical Association journal : IMAJ
Periodical, Abbrev.
Isr.Med.Assoc.J.
Pub Date Free Form
Jul
Volume
3
Issue
7
Start Page
504
Other Pages
507
Notes
LR: 20061115; JID: 100930740; ppublish
Place of Publication
Israel
ISSN/ISBN
1565-1088
Accession Number
PMID: 11791417
Language
eng
SubFile
Comparative Study; Journal Article; Research Support, Non-U.S. Gov't; IM
DOI
Output Language
Unknown(0)
PMID
11791417
Abstract
BACKGROUND: Prevention of cigarette smoking is an important issue in public health policy. Since most adult smokers began smoking in childhood, understanding behavorial factors associated with smoking initiation would contribute to smoking initiation programs. Health-related behavior may vary between different ethnic groups. OBJECTIVES: To determine the prevalence of smoking among Jewish and Arab adolescents in Jerusalem, and whether there are differences in smoking initiation between the two ethnic groups. METHODS: We carried out a cross-sectional survey of all students in the 6th to 11th grades (age range 11-17 years) of a Jewish school and an Arab school in the Jerusalem area, using an anonymous self-completion questionnaire. A total of 791 questionnaires was analyzed, 479 from the Jewish students and 312 from the Arab students. RESULTS: The lowest prevalence of smoking was found among Arab female students and the highest among Jewish female students (9% vs. 41%, P < 0.001). The prevalence of smoking among Jewish and Arab males was similar. More Arab female students smoked than their mothers. Peer pressure seemed to be a more important factor among Jewish students. CONCLUSIONS: This study demonstrated the presence of ethnic differences in smoking prevalence and the reasons for smoking among adolescents in Israel. These results suggest the need for specific smoking prevention policies for different ethnic groups.
Descriptors
Adolescent, Adolescent Behavior/ethnology/psychology, Age Distribution, Arabs/psychology/statistics & numerical data, Child, Cross-Sectional Studies, Female, Health Behavior/ethnology, Health Surveys, Humans, Israel/epidemiology, Jews/psychology/statistics & numerical data, Male, Sex Distribution, Smoking/ethnology/psychology, Smoking Cessation/ethnology/psychology
Links
Book Title
Database
Publisher
Data Source
Authors
Meijer,B., Branski,D., Kerem,E.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Ethnic and gender differences in smoking and smoking cessation in a population of young adult air force recruits 2002 University of Memphis Center for Community Health, 5050 Poplar Avenue, Suite 1800, Memphis, TN 38157, USA.
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
American Journal of Health promotion : AJHP
Periodical, Abbrev.
Am.J.Health Promot.
Pub Date Free Form
May-Jun
Volume
16
Issue
5
Start Page
259
Other Pages
266
Notes
LR: 20151119; GR: HL-53478/HL/NHLBI NIH HHS/United States; JID: 8701680; ppublish
Place of Publication
United States
ISSN/ISBN
0890-1171; 0890-1171
Accession Number
PMID: 12053437
Language
eng
SubFile
Comparative Study; Journal Article; Research Support, U.S. Gov't, P.H.S.; T
DOI
Output Language
Unknown(0)
PMID
12053437
Abstract
PURPOSE: To examine gender and ethnic differences in smoking and smoking cessation in a population of young adult military recruits. DESIGN: A self-administered survey of demographics, tobacco use, and other health risk behaviors was administered at the start of basic military training. SETTING: The study was conducted at Lackland Air Force Base, San Antonio, Texas, where all U.S. Air Force recruits complete basic military training. SUBJECTS: All recruits who entered the U.S. Air Force between September 1995 and September 1996 participated in this study (n = 32,144; 100% participation rate). MEASURES: Recruits completed a written 53-item behavioral risk questionnaire. Measures examined in the present study included smoking status (ever having smoked a cigarette, current daily smoking, and quitting); demographics (ethnicity, gender, education, family income, and age); smoking history; and nicotine dependence. RESULTS: Rates of ever smoking, current daily smoking, and quitting were examined in multiple logistic regression analyses as a function of gender and ethnicity, controlling for age, education, and family income. Overall, 54% of recruits had ever smoked a cigarette and 24.9% smoked daily at the time of entry into basic military training. Smoking rates were highest among white and Native American recruits. Among whites, women were more likely to be a current daily smoker (31.6% vs. 29.4%; odds ratio [OR] = 1.18, 99% confidence intervals [CI] = 1.08-1.29). The opposite pattern was observed among African-Americans (5.6% vs. 9.8%, respectively; OR = .57; CI = .41-.79). Current smokers had low levels of nicotine dependence compared with the general population of U.S. smokers, but whites tended to be more dependent than other ethnic groups. Cessation rates were similar for men and women but differed according to ethnicity, ranging from 15% among whites to 23% among Hispanics. CONCLUSIONS: These findings document important gender and ethnic differences in cigarette smoking among military recruits. Whites and Native Americans were more likely to smoke, less likely to quit, and more nicotine-dependent than other ethnic groups. Across gender/ethnicity groups, smoking rates were especially high among white women, with nearly one-third smoking daily until entry into basic training. Gender differences were not observed in cessation rates, but Hispanics were more likely than other ethnic groups to have quit smoking. The results highlight the need to develop effective cessation interventions for this population.
Descriptors
Adolescent, Adult, Ethnic Groups/psychology, Female, Humans, Male, Military Personnel/psychology, Prevalence, Risk-Taking, Sex Factors, Smoking/epidemiology/ethnology, Smoking Cessation/ethnology/statistics & numerical data, Surveys and Questionnaires, Texas/epidemiology, Tobacco Use Disorder
Links
Book Title
Database
Publisher
Data Source
Authors
Ward,K. D., Vander Weg,M. W., Kovach,K. W., Klesges,R. C., DeBon,M. W., Haddock,C. K., Talcott,G. W., Lando,H. A.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Etching enamel for orthodontics with an erbium, chromium:yttrium-scandium-gallium-garnet laser system 2007 Dicle University, Orthodontics, Faculty of Dentistry, Campus, Diyarbakir, Turkey. basaran@dicle.edu.tr
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
The Angle Orthodontist
Periodical, Abbrev.
Angle Orthod.
Pub Date Free Form
Jan
Volume
77
Issue
1
Start Page
117
Other Pages
123
Notes
LR: 20131121; JID: 0370550; 0 (Phosphoric Acids); 0R0008Q3JB (Chromium); 77B218D3YE (Erbium); E4GA8884NN (phosphoric acid); 2005/12/01 [received]; 2006/01/01 [accepted]; ppublish
Place of Publication
United States
ISSN/ISBN
0003-3219; 0003-3219
Accession Number
PMID: 17029548
Language
eng
SubFile
Comparative Study; Evaluation Studies; Journal Article; D; IM
DOI
10.2319/120605-426R.1 [doi]
Output Language
Unknown(0)
PMID
17029548
Abstract
OBJECTIVE: To test the shear bond strength, surface characteristics, and fracture mode of brackets that are bonded to enamel etched with an erbium, chromium:yttrium-scandium-gallium-garnet (Er,Cr:YSGG) laser operated at different power outputs: 0.5 W, 1 W, and 2 W. MATERIALS AND METHODS: Human premolars that had been extracted for orthodontic purposes were used. Enamel was etched with an Er,Cr:YSGG laser system operated at one of three power outputs or with orthophosphoric acid. RESULTS: The shear bond strength associated with the 0.5-W laser irradiation was significantly less than the strengths obtained with the other irradiations. Both the 1-W and 2-W laser irradiations were capable of etching enamel in the same manner. This finding was confirmed by scanning electron microscopy examination. The evaluation of adhesive-remnant-index scores demonstrated no statistically significant difference in bond failure site among the groups, except for the 0.5-W laser-etched group. Generally, more adhesive was left on the enamel surface with laser irradiation than with acid etching. CONCLUSION: The mean shear bond strength and enamel surface etching obtained with an Er,Cr: YSGG laser (operated at 1 W or 2 W for 15 seconds) is comparable to that obtained with acid etching.
Descriptors
Analysis of Variance, Bicuspid, Chi-Square Distribution, Chromium, Dental Bonding, Dental Debonding, Dental Enamel, Dental Etching/methods, Dental Stress Analysis, Erbium, Humans, Lasers, Microscopy, Electron, Scanning, Phosphoric Acids, Shear Strength, Surface Properties
Links
Book Title
Database
Publisher
Data Source
Authors
Basaran,G., Ozer,T., Berk,N., Hamamci,O.
Original/Translated Title
URL
Date of Electronic
PMCID
Editors
Estimating the beginning of the waterpipe epidemic in Syria 2004
Source Type
Print(0)
Ref Type
Journal Article
Periodical, Full
BMC Public Health
Periodical, Abbrev.
BMC Public Health
Pub Date Free Form
Volume
4
Issue
Start Page
32
Other Pages
32
Notes
ID: 15294023
Place of Publication
ISSN/ISBN
Accession Number
Language
en
SubFile
DOI
Output Language
Unknown(0)
PMID
Abstract
BACKGROUND: Waterpipe smoking is becoming a global public health problem, especially in the Eastern Mediterranean region (EMR). METHODS: We try in this study, which is a cross sectional survey among a representative sample of waterpipe smokers in cafes/restaurants in Aleppo-Syria, to assess the time period for the beginning of this new smoking hype. We recruited 268 waterpipe smokers (161 men, 107 women; mean age +/- standard deviation (SD) 30.1 +/- 10.2, response rate 95.3%). Participants were divided into 4 birth cohorts (1980) and year of initiation of waterpipe smoking and daily cigarette smoking were plotted according to these birth cohorts. RESULTS: Data indicate that unlike initiation of cigarette smoking, which shows a clear age-related pattern, the nineties was the starting point for most of waterpipe smoking implicating this time period for the beginning of the waterpipe epidemic in Syria. CONCLUSION: The introduction of new flavored and aromatic waterpipe tobacco (Maassel), and the proliferation of satellite and electronic media during the nineties may have helped spread the new hype all over the Arab World.
Descriptors
Health Knowledge, Attitudes, Practice, Smoking/epidemiology, Social Perception, Adolescent, Adult, Cross-Sectional Studies, Female, Humans, Male, Middle Aged, Restaurants, Sex Factors, Smoking/psychology, Socioeconomic Factors, Syria/epidemiology, Water
Links
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC514554/?tool=pubmed
Book Title
Database
MEDLINE; http://www.globalhealthlibrary.net/
Publisher
Data Source
Authors
Rastam,Samer, Ward,Kenneth D., Eissenberg,Thomas, Maziak,Wasim
Original/Translated Title
URL
Date of Electronic
PMCID
Editors